CODE 65111 ACADEMIC YEAR 2016/2017 CREDITS 7 cfu anno 2 CHIMICA E TECNOLOGIE CHIMICHE 8757 (L-27) - SCIENTIFIC DISCIPLINARY SECTOR CHIM/06 TEACHING LOCATION SEMESTER Annual PREREQUISITES Propedeuticità in ingresso Per sostenere l'esame di questo insegnamento è necessario aver sostenuto i seguenti esami: Chemistry and Chemical Technologies 8757 (coorte 2015/2016) ORGANIC CHEMISTRY 65100 2015 Propedeuticità in uscita Questo insegnamento è propedeutico per gli insegnamenti: Chemistry and Chemical Technologies 8757 (coorte 2015/2016) CHEMISTRY OF NATURAL ORGANIC SUBSTANCES 34000 Chemistry and Chemical Technologies 8757 (coorte 2015/2016) APPLIED ORGANIC CHEMISTRY 34767 Chemistry and Chemical Technologies 8757 (coorte 2015/2016) BIOORGANIC CHEMISTRY 34001 AIMS AND CONTENT SYLLABUS/CONTENT Basic safety principles in the organic chemistry laboratory. How to keep a notebook. Methods for separation and purification of organic compounds, including basic theoretical principles: extraction, crystallization, distillation (simple, fractional, reduced pressure distillation, steam distillation, azeotropes), sublimation, column chromatography, thin layer chromatography. Analytical methods: melting point, optical rotation power. Redox reactions in organic chemistry: how to balance them. Description of the laboratory experiments: theory of the reactions and, in particular, practical aspects of the laboratory procedures will be surveyed. Laboratory experiments on purification methods and on syntheses of compounds. Determination of melting points, optical rotation power, diastereomeric ratio through gas chromatopgraphy coupled with MS or FID. Recording of IR and NMR spectra of the prepared compounds. TEACHERS AND EXAM BOARD RENATA RIVA Exam Board RENATA RIVA (President) LUCA BANFI FERNANDO SANCASSAN EXAMS Exam schedule Data appello Orario Luogo Degree type Note 22/06/2017 09:00 GENOVA Scritto 22/06/2017 09:00 GENOVA Scritto + Orale 22/06/2017 10:30 GENOVA Scritto 20/07/2017 09:00 GENOVA Scritto + Orale 20/07/2017 09:00 GENOVA Scritto 20/07/2017 10:30 GENOVA Scritto 07/09/2017 09:00 GENOVA Scritto 07/09/2017 09:00 GENOVA Scritto + Orale 07/09/2017 10:30 GENOVA Scritto 21/09/2017 09:00 GENOVA Scritto + Orale 21/09/2017 09:00 GENOVA Scritto 21/09/2017 10:30 GENOVA Scritto