CODE 65111 ACADEMIC YEAR 2019/2020 CREDITS 7 cfu anno 2 CHIMICA E TECNOLOGIE CHIMICHE 8757 (L-27) - GENOVA SCIENTIFIC DISCIPLINARY SECTOR CHIM/06 LANGUAGE Italian TEACHING LOCATION GENOVA SEMESTER Annual PREREQUISITES Propedeuticità in ingresso Per sostenere l'esame di questo insegnamento è necessario aver sostenuto i seguenti esami: Chemistry and Chemical Technologies 8757 (coorte 2018/2019) ORGANIC CHEMISTRY 65100 2018 Propedeuticità in uscita Questo insegnamento è propedeutico per gli insegnamenti: Chemistry and Chemical Technologies 8757 (coorte 2018/2019) BIOORGANIC CHEMISTRY 34001 Chemistry and Chemical Technologies 8757 (coorte 2018/2019) CHEMISTRY OF NATURAL ORGANIC SUBSTANCES 34000 Chemistry and Chemical Technologies 8757 (coorte 2018/2019) APPLIED ORGANIC CHEMISTRY 34767 TEACHING MATERIALS AULAWEB AIMS AND CONTENT SYLLABUS/CONTENT Basic safety principles in the organic chemistry laboratory. How to keep a notebook. Methods for separation and purification of organic compounds, including basic theoretical principles: extraction, crystallization, distillation (simple, fractional, reduced pressure distillation, steam distillation, azeotropes), sublimation, column chromatography, thin layer chromatography. Analytical methods: melting point, optical rotation power. Redox reactions in organic chemistry: how to balance them. Description of the laboratory experiments: theory of the reactions and, in particular, practical aspects of the laboratory procedures will be surveyed. Laboratory experiments on purification methods and on syntheses of compounds. Determination of melting points, optical rotation power, diastereomeric ratio through gas chromatopgraphy coupled with MS or FID. Recording of IR and NMR spectra of the prepared compounds. TEACHERS AND EXAM BOARD RENATA RIVA Ricevimento: I'm available every day of the week. Please, contact me before by e-mail for an appointment. Exam Board RENATA RIVA (President) LUCA BANFI LARA BIANCHI CHIARA LAMBRUSCHINI LISA MONI EXAMS Exam schedule Data appello Orario Luogo Degree type Note 23/01/2020 09:00 GENOVA Scritto + Orale 13/02/2020 09:00 GENOVA Scritto + Orale 18/06/2020 09:00 GENOVA Scritto + Orale 16/07/2020 09:00 GENOVA Scritto + Orale 03/09/2020 09:00 GENOVA Scritto + Orale 17/09/2020 09:00 GENOVA Scritto + Orale