CODE 94830 ACADEMIC YEAR 2017/2018 CREDITS 3 cfu anno 1 SCIENZA E INGEGNERIA DEI MATERIALI 9017 (LM-53) - SCIENTIFIC DISCIPLINARY SECTOR CHIM/03 LANGUAGE English TEACHING LOCATION SEMESTER 2° Semester OVERVIEW Understanding the fundamentals of microscopy techniques and interrelated spectroscopies, in investigation of materials. AIMS AND CONTENT LEARNING OUTCOMES Understanding the fundamentals of electron microscopies and energy dispersive x-ray spectroscopy, which permit the observation and characterization of heterogeneous organic and inorganic materials. TEACHING METHODS Lectures SYLLABUS/CONTENT Scanning electron microscopy and microprobe: electron optics, electron beam - specimen interaction, signal detection, image formation, contrast types. EDX and WDX spectroscopy; qualitative and quantitative x-ray analysis. Transmission electron microscopy: elastic and inelastic scattering phenomena. The microscope: the illumination system, the objective lens and stage, the imaging system. Introduction to the different types of contrast. Introduction to electron diffraction. Sample preparation techniques. RECOMMENDED READING/BIBLIOGRAPHY “Scanning Electron Microscopy and X-ray Microanalysis”, J.I. Goldstein, D.E. Newbury, P. Echlin, D.C. Joy, A.D. Romig, Jr., C.E. Lyman, C. Fiori, E. Lifshin, Plenum Press, 1992. “Trasmission Electron Microscopy”, D.B. Williams and C.B. Carter, Plenum Press, 1996. TEACHERS AND EXAM BOARD PAOLA RIANI Ricevimento: every day by appointment Exam Board PAOLA RIANI (President) ANDREA BASSO GABRIELE CACCIAMANI LESSONS LESSONS START Second semester Class schedule The timetable for this course is available here: Portale EasyAcademy EXAMS EXAM DESCRIPTION Written exam ASSESSMENT METHODS Student have to answer to 3 or 4 questions on the topics discussed in the course. In addition on student request, a short oral exam can also be supported. Exam schedule Data appello Orario Luogo Degree type Note 18/06/2018 19:00 GENOVA Orale 02/07/2018 19:00 GENOVA Orale 07/09/2018 19:00 GENOVA Orale 21/09/2018 19:00 GENOVA Orale