CODE 65375 ACADEMIC YEAR 2022/2023 CREDITS 9 cfu anno 1 SCIENZA DEI MATERIALI 8765 (L-30) - GENOVA SCIENTIFIC DISCIPLINARY SECTOR CHIM/03 LANGUAGE Italian TEACHING LOCATION GENOVA SEMESTER 2° Semester PREREQUISITES Propedeuticità in ingresso Per sostenere l'esame di questo insegnamento è necessario aver sostenuto i seguenti esami: Material Science 8765 (coorte 2022/2023) GENERAL AND INORGANIC CHEMISTRY WITH LABORATORY 65847 2022 TEACHING MATERIALS AULAWEB AIMS AND CONTENT AIMS AND LEARNING OUTCOMES Acquire good command in the evaluation of the properties of inorganic compounds and in the knowledge of the main analytical techniques with particular reference to their applications in the field of materials. PREREQUISITES Knowledge of General Chemistry TEACHING METHODS Teaching organization The classic lectures (which include exercises aimed at verifying the state of learning) are alternated with innovative teaching methods aimed at active and collaborative learning by students, to make teaching, with equal efficacy, more engaging and captivating. The laboratory experiences are intended to experimentally verify some aspects of classical and instrumental analytical chemistry. SYLLABUS/CONTENT Program: Inorganic chemistry Completion of knowledge on chemical bond, metallic bond - Ionic, metallic, molecular, covalent solids - Structure of elementary substances - Some classes of the main inorganic compounds (oxides, hydrides, hydroxides, oxides, halides) and variation of their properties in the periodic system - Silicate structure and nod to inorganic silicate-based materials - Phase equilibria in heterogeneous systems, some of the most significant state diagrams in the context of liquid-solid binary systems - Preparation of metals by reduction processes, thermodynamic aspects, Ellingham- Preparation of metals with electrolytic processes- Methods of purification of metals: -Preparation, purification and properties of some important metals (Cu, Al, Ti) Analytical Chemistry Sampling.- Classical quantitative analysis. - Instrumental analytical chemistry: chromatographic and optical spectroscopy techniques RECOMMENDED READING/BIBLIOGRAPHY Reference texts Inorganic Chemistry: During the course, educational material will be published (Aul @ WEB), but integration with appropriate texts is essential. Any text at university level of "General Chemistry" commercially available or available in the library of the School of Sciences M.F.N. it is valid, provided it is recent (from this century). For each student it is more useful and productive to search, for each topic, the text in which the didactic approach is more appreciated and stimulating, rather than relying on a single textbook. Having said that, and bearing in mind that the list below is certainly not exhaustive, some titles, a non-binding selection of texts, are as follows: Atkins, Jones, Laverman - PRINCIPI DI CHIMICA ‐ Zanichelli Atkins - FONDAMENTI DI CHIMICA GENERALE ‐ Zanichelli Kotz, Treichel, Weaver ‐ CHIMICA - EdiSES Kotz ∙ Treichel ∙ Townsend ∙ Treichel ‐ CHIMICA ‐ EdiSES Manotti Lanfredi , Tiripicchio FONDAMENTI DI CHIMICA ‐ CEA Milano Petrucci, Herring, Bissonnette ‐ CHIMICA GENERALE ‐ Piccin Petrucci, Herring, Madura, Bissonnette CHIMICA GENERALE ‐ Piccin Silberberg ‐ CHIMICA 1° o 2° ed. ‐ McGraw‐Hill Whitten, Davis, Speck, Stanley ‐ CHIMICA ‐ Piccin Bertini, Luchinat, Mani – CHIMICA INORGANICA- EdiSES Atkins et al. - CHIMICA INORGANICA ‐ Zanichelli To know more: Chiorboli - FONDAMENTI DI CHIMICA - UTET Greenwood , Earnshaw - CHIMICA DEGLI ELEMENTI - Piccin Callister, Rethwisch - SCIENZA ED INGEGNERIA DEI MATERIALI - EdiSES Analytical Chemistry: Skoog, West, Holler - Fondamentri di Chimica analitica - EdiSES K.A.Rubinson, J.F.Rubinson - Chimica Analitica Strumentale - Zanichelli Recommended texts: Fondamenti di Chimica Analitica quantitativa, Daniel C. Harris, ed. Zanichelli, 2017 Analisi statistica dei dati biologici, Michael C. Whitlock, Dolph Schluter, ed. Zanichelli, 2010 TEACHERS AND EXAM BOARD NADIA PARODI Ricevimento: By appointment. email: nadia.parodi@unige.it RICCARDO NARIZZANO Exam Board NADIA PARODI (President) RICCARDO NARIZZANO (President Substitute) LESSONS LESSONS START Start and end dates and calendar of educational activities see poster on the website and timetable on the website https://servizionline.unige.it/unige/stampa_manifesto/MF/2022/8765.html Class schedule INORGANIC AND ANALYTICAL CHEMISTRY EXAMS EXAM DESCRIPTION Evaluation methods the exam consists of a written test and an oral test to verify the achievement of the training objectives Prerequisites: the examination of general and inorganic chemistry with laboratory is preparatory ASSESSMENT METHODS The written test consists of exercises similar to those faced during the course and descriptive questions both for the part of inorganic chemistry and for that of analytical chemistry. The oral test, reserved for students who have successfully completed the written test (≥18 / 30), is public. The interview aims to ascertain the possession of knowledge and the level of deepening of the subject achieved by the student. The final, single mark is calculated as the average of the written and oral tests as well as the assessment of laboratory experiences and the evaluation of the relative reports. The oral exam is always carried out by the teaching staff. Exam schedule Data Ora Luogo Degree type Note 19/01/2023 14:00 GENOVA Scritto 02/02/2023 14:00 GENOVA Scritto 21/06/2023 14:00 GENOVA Scritto 12/07/2023 14:00 GENOVA Scritto 20/09/2023 09:00 GENOVA Scritto